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Kyiv, Ukraine, 22 November 2021. Recently, Prof. Magolan and coworkers from McMaster University (Hamilton, Ontario, Canada) reported that hexafluoroisopropyl sulfamate (HFIPS) is a convenient reagent for the sulfamoylation of alcohols and amines (Org. Lett. 2021, 23, 3373–3378). HFIPS has likewise been used for metallic-catalyzed C–H aminations (J. Am. Chem. Soc. 2014, 136, 5783–5789) and for the synthesis of aziridines using silver catalysis (Synthesis 2018, l, 4462–4470) or electrochemical conditions (Angew. Chem. Int. Ed. 2018, 57, 5695–5698). Enamine has adapted and scaled-up the published procedure to synthesize HFIPS and make it more than accessible to scientists worldwide. The reagent is now available in Enamine'south catalogue in multigram quantities.
Iryna Iavniuk, Business Evolution Director at Enamine, comments: "We at Enamine are committed to making novel reagents immediately accessible to our customers. Nosotros have successfully applied the HFIPS reagent in one of our projects previously and were happy to produce it for commercialization."
Prof. Dr. Oleksandr Grygorenko, Consulting Scientist at Enamine, explains: "Dr. Jarrod Johnson, a Research Associate in the Magolan group, contacted us to point out that there was a supply gap with HFIPS. We recognized the usefulness of the reagent and happily agreed to begin commercialization. Our chemists quickly reproduced the published process to synthesize 50 grams of the reagent and HFIPS is at present available from EnamineStore: https://www.enaminestore.com/catalog/EN300-1987789."
Dr. Jarrod Johnson from McMaster Academy, adds: "We like the ease and simplicity of using HFIPS for sulfamoylation chemistry and promise information technology might become the go-to reagent for medicinal chemists making sulfamates and sulfamides."
Prof. Dr. Jakob Magolan from McMaster University, comments: "It'southward great to see Enamine at present offering majority HFIPS. I look that this will enable artistic scientists around the globe to further extend the scope and applicability of this useful little reagent."
Conflict of interest statement: Hereby the parties ostend that Prof. Magolan and his group have no financial involvement in commercialization of EN300-1987789. No specialized data was transferred to Enamine apart from that already published in the literature.
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Source: https://enamine.net/
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